HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86598889, compound → HCID 86598888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86598889 | HCID 86598889 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86598888 | HCID 86598888 | — |
Reaction Steps
To a solution of ethyl (1S,3S,4S,5R)-5-hydroxy-2-[(1R)-1-phenylethyl]-2-azabicyclo[2.2.2]octane-3-carboxylate obtained in Example 2-3 (22 g) in ethanol (300 mL), was added Pearlman's catalyst (4 g). The mixture was stirred for 3 hrs under H2 atmosphere on 4 atm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07186731B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-e9958ddb92244f639781a28cfb10d9cb |
| Source note | uspto-grants-2007_03 |