HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10859068, compound → HCID 16228805, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10859068 | HCID 10859068 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 16228805 | HCID 16228805 | 99.1% |
Reaction Steps
A solution of ethyl (1S,3S,4R)-2-[(1R)-1-phenylethyl]-2-azabicyclo[2.2.2]oct-5-ene-3-carboxylate (1.1 g) in ethanol (20 mL) was hydrogenated under H2 atmosphere (4 atm) for 2 hrs. After removal of the catalyst by filtration, the solvent was removed in vacuo to give the target compound as a colorless oil (700 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07186731B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-1118eef5711f4d568d1d402945cbd4db |
| Source note | uspto-grants-2007_03 |