HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-Bromo-3-(bromomethyl)benzoate → HCID 10185564, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-Bromo-3-(bromomethyl)benzoate | HCID 11460987 | — |
| Reactant | HCID 17964331 | HCID 17964331 | — |
| Product | HCID 10185564 | HCID 10185564 | — |
Reaction Steps
This compound was prepared following the procedure described in example 13 (part D) starting with 1.5 g (50 mmol) of 3-piperidin-4-yl-1-pyridin-4-ylmethyl-1H-indole and 1.7 g (55 mmol) of 4-bromo-3-bromomethyl-benzoic acid methyl ester. After standard work-up and recrystallisation with ethyl ether, 1.7 g (68% of yield) of the expected acid were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07189741B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-04e5b194cdf44f03bd2fe2f591eeff6c |
| Source note | uspto-grants-2007_03 |