HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-(bromomethyl)-4-methoxybenzoate → HCID 17964360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-(bromomethyl)-4-methoxybenzoate | HCID 139928 | — |
| Reactant | HCID 17964350 | HCID 17964350 | — |
| Product | HCID 17964360 | HCID 17964360 | — |
Reaction Steps
This compound was prepared following the procedure described in example 13 (part D) starting with 0.05 g (0.17 mmol) of 1-furan-2-ylmethyl-5-methoxy-3-piperidin-4-yl-1H-indole and 0.057 g (0.22 mmol) of 2-bromomethyl-4-methoxy-benzoic acid methyl ester. After standard work-up and purification by chromatography using a C18 column, 0.029 g (36% of yield) of the expected acid were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07189741B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-26d3354d0b5d4bf09777bcbbb4a7faec |
| Source note | uspto-grants-2007_03 |