HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17964375, compound → HCID 17964319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17964375 | HCID 17964375 | — |
| Reactant | 5-Bromomethyl-2-methoxybenzoic acid ethyl ester | HCID 68893946 | — |
| Product | HCID 17964319 | HCID 17964319 | — |
Reaction Steps
This compound was prepared following the procedure described in example 13 (part D) starting with 0.1 g (0.38 mmol) of 3-piperidin-4-yl-1-thiophen-3-ylmethyl-1H-indole and 0.13 g (0.48 mmol) of 5-bromomethyl-2-methoxy-benzoic acid ethyl ester. The crude mixture was purified by HPLC-MS using a C-18 column, and 0.002 g (94% of purity) of the expected acid were isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07189741B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-b1a41f63c5f84c8e8c9164c6e88f2475 |
| Source note | uspto-grants-2007_03 |