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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 457868Generated: November 3, 2026

HCID 17964369, compound → HCID 17964297, compound

https://huagongshe.com/reaction/457868

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 17964369HCID 17964369—
Reactant5-Bromomethyl-2-methoxybenzoic acid ethyl esterHCID 68893946—
ProductHCID 17964297HCID 17964297—

Reaction Steps

This compound was prepared following the procedure described in example 13 (part D) starting with 0.05 g (0.13 mmol) 1-(5-chloro-thiophen-2-ylmethyl)-5-methoxy-3-piperidin-4-yl-1H-indole and 0.05 g (0.18 mmol) of 5-bromomethyl-2-methoxy-benzoic acid ethyl ester. The crude mixture was purified by HPLC-MS using a C-18 column, and 0.002 g (99% of purity) of the expected acid were isolated.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07189741B2
Source datasetuspto-grants-2007_03
ORD IDord-64e3fa2b975a4b899f65b3b9bd3db022
Source noteuspto-grants-2007_03