HRID458134
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Methyl 4-acetamido-5-chloro-2-methoxybenzoate is stirred with aqueous sodium hydroxide until complete solution is achieved. After filtration, concentrated hydrochloric acid is added, whereupon, the product precipitates out as a white solid which is filtered off, washed and dried. 4-Acetamido-5-chloro-2-methoxybenzoic acid is crystallised from isopropanol, filtered off, washed and dried.
WORKUP
后处理
- filtrationAfter filtration, concentrated hydrochloric acid
- additionis added
- customwhereupon, the product precipitates out as a white solid which
- filtrationis filtered off
- washwashed
- customdried
- custom4-Acetamido-5-chloro-2-methoxybenzoic acid is crystallised from isopropanol
- filtrationfiltered off
- washwashed
- customdried