HRID458134

反应详情

EQUATION

反应方程式

HRID 458134 的结构方程式

PROCEDURE

实验过程

Methyl 4-acetamido-5-chloro-2-methoxybenzoate is stirred with aqueous sodium hydroxide until complete solution is achieved. After filtration, concentrated hydrochloric acid is added, whereupon, the product precipitates out as a white solid which is filtered off, washed and dried. 4-Acetamido-5-chloro-2-methoxybenzoic acid is crystallised from isopropanol, filtered off, washed and dried.

WORKUP

后处理

  1. filtrationAfter filtration, concentrated hydrochloric acid
  2. additionis added
  3. customwhereupon, the product precipitates out as a white solid which
  4. filtrationis filtered off
  5. washwashed
  6. customdried
  7. custom4-Acetamido-5-chloro-2-methoxybenzoic acid is crystallised from isopropanol
  8. filtrationfiltered off
  9. washwashed
  10. customdried