HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 4-Acetamido-5-chloro-2-methoxybenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 4-acetamido-5-chloro-2-methoxybenzoate | HCID 77721 | — |
| Product | 4-Acetamido-5-chloro-2-methoxybenzoic acid | HCID 10988496 | — |
Reaction Steps
Methyl 4-acetamido-5-chloro-2-methoxybenzoate is stirred with aqueous sodium hydroxide until complete solution is achieved. After filtration, concentrated hydrochloric acid is added, whereupon, the product precipitates out as a white solid which is filtered off, washed and dried. 4-Acetamido-5-chloro-2-methoxybenzoic acid is crystallised from isopropanol, filtered off, washed and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07189852B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-8a0bdea1b1f342208709bca597f240c8 |
| Source note | uspto-grants-2007_03 |