HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 458486Generated: October 30, 2026
Oxalyl chloride → HCID 12554870, compound
https://huagongshe.com/reaction/458486
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 12554866 | HCID 12554866 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 12554870 | HCID 12554870 | — |
Reaction Steps
With stirring at 50° C., 60.0 g of oxalyl chloride was slowly added dropwise to a mixture of 69.8 g of 2-(trimethylsilylmethyl)acrylic acid obtained in Example 2 and 300 ml of toluene. Stirring was continued at the temperature. After gas evolution ceased, stirring was continued at 70° C. for 2 hours. After cooling, the product in toluene solution was directly used in the subsequent step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07192684B2 |
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| Source dataset | uspto-grants-2007_03 |
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| ORD ID | ord-e94cde806f554a2280a38e87b380357e |
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| Source note | uspto-grants-2007_03 |
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