1-Naphthalenemethanamine → HCID 18442578, compound

HRID 458814Notes

Reaction equation

Br[CH2:2][C:3](Br)=[O:4].[C:6]1([CH2:16][NH2:17])[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]=[CH:8][CH:7]=1.[CH3:18][O:19][C:20]1[CH:21]=[C:22]([CH:39]=[CH:40][C:41]=1[O:42][CH3:43])[CH2:23][CH:24]1[C:30]2[CH:31]=[C:32]([O:37][CH3:38])[C:33]([O:35][CH3:36])=[CH:34][C:29]=2[O:28][CH2:27][CH2:26][NH:25]1>>[CH3:18][O:19][C:20]1[CH:21]=[C:22]([CH:39]=[CH:40][C:41]=1[O:42][CH3:43])[CH2:23][CH:24]1[C:30]2[CH:31]=[C:32]([O:37][CH3:38])[C:33]([O:35][CH3:36])=[CH:34][C:29]=2[O:28][CH2:27][CH2:26][N:25]1[CH2:2][C:3]([NH:17][CH2:16][C:6]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]=[CH:8][CH:7]=1)=[O:4]

Participants

Reactant 3

HCID 83551-Naphthalenemethanamine

HCID 61147Bromoacetyl bromide

HCID 184425855-(3,4-Dimethoxy-benzyl)-7,8-dimethoxy-2,3,4,5-tetrahydro benzo[f][1,4]oxazepine

Product 1

HCID 18442578HCID 18442578, compound

Procedure

prepared by reaction of 2-bromoacetyl bromide with 1-naphtalenemethylamine and 5-(3,4-dimethoxy-benzyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine.

Sources & evidence

ORD record: ord-b43fe4eeba2d4c5faf129d64ef0270b3
Source dataset: uspto-grants-2007_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07192950B2

Reaction notes

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