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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 458878Generated: November 1, 2026

Oxalyl chloride → HCID 57083494, compound

https://huagongshe.com/reaction/458878

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
Reactant3-(3-Pyridinyl)-2-propenoic acidHCID 101984—
ReactantHCID 53758378HCID 53758378—
ProductHCID 57083494HCID 57083494—

Reaction Steps

Batch size: 5.3 g (35.5 mmol) 3-(3-pyridyl)-acrylic acid, 12.4 g (97.9 mmol) oxalyl chloride and 8.6 g (32.6 mmol) 6-(1,3-dioxo-1H, 3H-benzo[de]isoquinolin-2-yl)-hexylamine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07192967B1
Source datasetuspto-grants-2007_03
ORD IDord-9483434bcc1e4f8b989d4add147452c1
Source noteuspto-grants-2007_03