Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 458879Generated: October 30, 2026

Oxalyl chloride → HCID 68501739, compound

https://huagongshe.com/reaction/458879

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
Reactant3-(3-Pyridinyl)-2-propenoic acidHCID 101984—
Reactant2-(2-aMinoethyl)-1H-benzo[de]isoquinoline-1,3(2H)-dioneHCID 11096719—
ProductHCID 68501739HCID 68501739—

Reaction Steps

Batch size: 7.5 g (50.4 mmol) 3-(3-pyridyl)-acrylic acid, 17.4 g (137.4 mmol) oxalyl chloride and 11.0 g (45.8 mmol) 2-(1,3-dioxo-1H, 3H-benzo[de]isoquinolin-2-yl)-ethylamine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07192967B1
Source datasetuspto-grants-2007_03
ORD IDord-834887655ef842afa70a10b852b40d1d
Source noteuspto-grants-2007_03