HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanepropanoic acid → HCID 178526602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanepropanoic acid | HCID 69702 | — |
| Reactant | 2-Bromo-1-(3-nitrophenyl)ethan-1-one | HCID 75213 | — |
| Reactant | N-(tert-butoxycarbonyl)glycine | HCID 78288 | — |
| Reactant | 4-Azidophenacyl bromide | HCID 92627 | — |
| Product | HCID 178526602 | HCID 178526602 | 26% |
Reaction Steps
This compound is prepared according to an operating method analogous to that described for Stage 4.1 of Example 4, with cyclohexylethylcarboxylic acid and 3-nitrophenacyl bromide placing N-(tert-butoxycarbonyl)-glycine and 4-azidophenacyl bromide respectively. The expected compound is obtained in the form of a yellow powder with a yield of 26%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192975B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-888ec7bdd9894376a72ebe9c688b6941 |
| Source note | uspto-grants-2007_03 |