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HRID458960

反应详情

EQUATION

反应方程式

HRID 458960 的结构方程式

REACTANTS

反应物

4
结构：O=C(O)CCC1CCCCC1
HCID69702

Cyclohexanepropionic acid

C9H16O2

结构：O=C(CBr)c1cccc([N+](=O)[O-])c1
HCID75213

2-Bromo-1-(3-nitrophenyl)ethan-1-one

C8H6BrNO3

结构：CC(C)(C)OC(=O)NCC(=O)O
HCID78288

Glycine, N-[(1,1-dimethylethoxy)carbonyl]-

C7H13NO4

结构：[N-]=[N+]=Nc1ccc(C(=O)CBr)cc1
HCID92627

4-Azidophenacyl bromide

C8H6BrN3O

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cccc(-c2c[nH]c(CCC3CCCCC3)n2)c1
HCID178526602

未命名化合物

收率 26%

PROCEDURE

实验过程

This compound is prepared according to an operating method analogous to that described for Stage 4.1 of Example 4, with cyclohexylethylcarboxylic acid and 3-nitrophenacyl bromide placing N-(tert-butoxycarbonyl)-glycine and 4-azidophenacyl bromide respectively. The expected compound is obtained in the form of a yellow powder with a yield of 26%.

WORKUP

后处理

  1. customThis compound is prepared