HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoromethanesulfonate → HCID 58822907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoromethanesulfonate | HCID 2758875 | — |
| Reactant | HCID 18443698 | HCID 18443698 | — |
| Reactant | HCID 58822780 | HCID 58822780 | — |
| Product | HCID 58822907 | HCID 58822907 | — |
Reaction Steps
The title compound was prepared from 6-But-3-ynyloxy-3-(4-fluoro-phenyl)-benzofuran and (2S)-2-methoxy-3-(4-trifluoromethanesulfonyloxy-phenyl)-propionic acid ethyl ester Example 1, Step A) following the procedure described in Example 40, Step C. The ethyl ester derivative was contaminated with starting triflate. The mixture was hydrolyzed using the Standard Procedure C. The residue was purified by chromatography. MS(ES) for C28H23FO5 [M−H]−: 457.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192982B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-f0df2f06000f467fa87dbc496e621e0b |
| Source note | uspto-grants-2007_03 |