HuagongsheHuagongshe Chemistry Print Report · For research reference only
Magnesium → 3-(3-Benzyloxy-phenyl)-2-methoxy-propionic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Magnesium | HCID 5462224 | — |
| Reactant | 3-(3-Benzyloxy-phenyl)-2-methoxy-acrylic acid methyl ester | HCID 69421755 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(3-Benzyloxy-phenyl)-2-methoxy-propionic acid methyl ester | HCID 58822620 | — |
Reaction Steps
Compound from Step B was dissolved in methanol and treated with magnesium. The flask was placed in an ice bath for 5 min and then the reaction mixture was stirred at room temperature for 4 hours. Washed with HCl 3N and extracted with ether. Dry and concentrated to dryness to get the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192982B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-c4d368ff1fa04e8099d31c20eac2a16a |
| Source note | uspto-grants-2007_03 |