HRID459171

反应详情

EQUATION

反应方程式

HRID 459171 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 3-(3-Benzyloxy-phenyl)-2-methoxy-propionic acid methyl ester in methanol was treated with a catalytic amount of C—Pd (0.1 eq) and then H2 was bubbled through the mixture and stirred overnight. The mixture reaction was concentrated and reconstituted in ethyl acetate, filtered through a pad of celite and concentrated in vacuo to give the title compound.

WORKUP

后处理

  1. customH2 was bubbled through the mixture
  2. customThe mixture reaction
  3. concentrationwas concentrated
  4. filtrationfiltered through a pad of celite
  5. concentrationconcentrated in vacuo