HRID459171
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of 3-(3-Benzyloxy-phenyl)-2-methoxy-propionic acid methyl ester in methanol was treated with a catalytic amount of C—Pd (0.1 eq) and then H2 was bubbled through the mixture and stirred overnight. The mixture reaction was concentrated and reconstituted in ethyl acetate, filtered through a pad of celite and concentrated in vacuo to give the title compound.
WORKUP
后处理
- customH2 was bubbled through the mixture
- customThe mixture reaction
- concentrationwas concentrated
- filtrationfiltered through a pad of celite
- concentrationconcentrated in vacuo