HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(3-Benzyloxy-phenyl)-2-methoxy-propionic acid methyl ester → 3-(3-Hydroxy-phenyl)-2-methoxy-propionic acid methyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(3-Benzyloxy-phenyl)-2-methoxy-propionic acid methyl ester | HCID 58822620 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 3-(3-Hydroxy-phenyl)-2-methoxy-propionic acid methyl ester | HCID 58822802 | — |
Reaktionsschritte
A solution of 3-(3-Benzyloxy-phenyl)-2-methoxy-propionic acid methyl ester in methanol was treated with a catalytic amount of C—Pd (0.1 eq) and then H2 was bubbled through the mixture and stirred overnight. The mixture reaction was concentrated and reconstituted in ethyl acetate, filtered through a pad of celite and concentrated in vacuo to give the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07192982B2 |
| Quelldatensatz | uspto-grants-2007_03 |
| ORD ID | ord-b007014497684df59673d529c516778b |
| Quellennotiz | uspto-grants-2007_03 |