HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Benzyloxy-3-methyl-phenyl)-2-methoxy-propionic acid ethyl ester → 3-(4-Hydroxy-3-methyl-phenyl)-2-methoxy-propionic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Benzyloxy-3-methyl-phenyl)-2-methoxy-propionic acid ethyl ester | HCID 69425304 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 3-(4-Hydroxy-3-methyl-phenyl)-2-methoxy-propionic acid ethyl ester | HCID 58822833 | — |
Reaction Steps
A solution of 3-(4-Benzyloxy-3-methyl-phenyl)-2-methoxy-propionic acid ethyl ester in ethyl acetate was treated with a catalytic amount of C—Pd (0.1 eq) and then H2 was bubbled through the mixture and stirred 2 hours. The mixture reaction was filtered through a pad of celite and concentrated in vacuo to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192982B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-2adc4350357a44c5a8aba22a3e04847d |
| Source note | uspto-grants-2007_03 |