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HRID459205

反应详情

EQUATION

反应方程式

HRID 459205 的结构方程式

REACTANTS

反应物

3
结构：OCCCOc1ccc(-c2ccccc2)cc1
HCID28351739

3-[([1,1'-Biphenyl]-4-yl)oxy]propan-1-ol

C15H16O2

结构：CCC(Cc1ccc(O)cc1OC)C(=O)OC
HCID69422796

未命名化合物

结构：CC(C)OC(=O)/N=N/C(=O)OC(C)C.Cc1ccccc1
HCID178459888

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(OCCCOc2ccc(-c3ccccc3)cc2)ccc1CC(OC)C(=O)O
HCID18443634

未命名化合物

PROCEDURE

实验过程

A mixture solution of 2-(4-hydroxy-2-methoxy-benzyl)-butyric acid methyl ester from Step C and 3-(biphenyl-4-yloxy)-propan-1-ol was reacted under the Standard Mitsounobu coupling conditions B (DIAD/toluene) to give the corresponding coupled product, which afforded the title compound via the Standard hydrolysis procedure C (NaOH). MS(ES) for C26H28O6 [M+NH4]+: 454.

WORKUP

后处理

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