HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl azodicarboxylate → HCID 69421933, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl azodicarboxylate | HCID 5363146 | — |
| Reactant | HCID 18443695 | HCID 18443695 | — |
| Reactant | HCID 58823028 | HCID 58823028 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 69421933 | HCID 69421933 | — |
Reaction Steps
(2S)-3-[4-(3-Hydroxy-propoxy)-phenyl)-2-methoxy-propionic acid ethyl ester and 4′-(tert-butyl-dimethyl-silanyloxy)-biphenyl-4-ol (Example 196, Step A) were treated under Mitsunobu procedure B (DIAD, toluene), to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192982B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-a18b349e154143eb9a3ff973fcf63967 |
| Source note | uspto-grants-2007_03 |