HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 426846, compound → HCID 58822564, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 426846 | HCID 426846 | — |
| Reactant | HCID 58822797 | HCID 58822797 | — |
| Product | HCID 58822564 | HCID 58822564 | — |
Reaction Steps
The title compound was prepared from (2S)-3-{4-[3-(4-hydroxy-phenoxy)-propoxy]-phenyl}-2-methoxy-propionic acid ethyl ester (Example 263, Step B) and methanesulfonic acid 3-dimethylaminopropyl ester (Step A) following the procedure described for Example 264. 1H-NMR (CDCl3, 200.15 MHz): δ 7.14 (d, 2H, J=7.8), 6.83–6.77 (m, 6H), 4.10–4.04 (m, 5H), 3.95–3.89 (m, 4H), 3.37 (s, 3H), 3.16–3.13 (m, 2H), 3.06–2.99 (m, 2H), 2.77 (s, 6H), 2.21–2.15 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192982B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-163f285d6d7b4bc8b325dd35cb1a1233 |
| Source note | uspto-grants-2007_03 |