HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Hydroxy-phenyl)-2-methoxy-propionic acid methyl ester → 3-[3-(2-Bromo-ethoxy)-phenyl]-2-methoxy-propionic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Hydroxy-phenyl)-2-methoxy-propionic acid methyl ester | HCID 58822802 | — |
| Reactant | (2S)-3-[4-(2-bromo-ethoxy)-phenyl]2-methoxy-propionic acid ethyl ester | HCID 58822865 | — |
| Product | 3-[3-(2-Bromo-ethoxy)-phenyl]-2-methoxy-propionic acid methyl ester | HCID 69423413 | — |
Reaction Steps
The title compound was prepared from 3-(3-hydroxy-phenyl)-2-methoxy-propionic acid methyl ester (Example 291, Step 4) (4.76 mol, 1000 mg) via the same procedure used for the preparation of (2S)-3-[4-(2-bromo-ethoxy)-phenyl]-2-methoxy-propionic acid ethyl ester (Example 283, Step 2). MS (ES) for C13H17BrO4 [M+NH4]+: 334:2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192982B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-ab5f517588c244968e71a8f7aea16185 |
| Source note | uspto-grants-2007_03 |