Hydrochloric Acid → HCID 68905633, compound

HRID 459505Notes

Reaction equation

HRID 459505 reaction equation
C(O[C:6]([N:8](C)[C@@H:9]1[CH2:14][CH2:13][CH2:12][CH2:11][C@@H:10]1[N:15](C(OC(C)(C)C)=O)[CH3:16])=O)(C)(C)C.[ClH:25]>C(O)C>[ClH:25].[CH3:6][NH:8][C@@H:9]1[CH2:14][CH2:13][CH2:12][CH2:11][C@@H:10]1[NH:15][CH3:16]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 58822047HCID 58822047, compound

Product 1

HCID 68905633HCID 68905633, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

cis-N1,N2-Bis(tert-butoxycarbonyl)-N1,N2-dimethyl-1,2-cyclohexanediamine (2.15 g) was dissolved in a saturated ethanol solution of hydrochloric acid, and the solution was stirred at room temperature for 30 minutes. The solvent was distilled off under reduced pressure, ethyl acetate was added to the residue, and solids were collected by filtration to obtain the title compound (1.19 g) as a pale yellow solid.

Workup

  1. distillationThe solvent was distilled off under reduced pressure, ethyl acetate
  2. additionwas added to the residue, and solids
  3. filtrationwere collected by filtration

Sources & evidence

ORD record
ord-7b1326088e1842be88491bb624fbc1ec
Source dataset
uspto-grants-2007_03
Patent number
US07192968B2

Reaction notes

Loading…