Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 131726306 | HCID 131726306 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178511000 | HCID 178511000 | 209% |
Reaction Steps
Following a method similar to example 1, 110 ml of water was added, raised the temperature up to 65° C. with stirring, added 25 g of lysine-glutamate, when dissolved completely, 3.0 g of fumaric acid was added, and 9.7 g of iodine was then introduced gradually, and the mixture was stirred for about 220 minutes, then filtrated, the filtrate was concentrated and dried to afford 33.4 g title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07195772B2 |
|---|
| Source dataset | uspto-grants-2007_03 |
|---|
| ORD ID | ord-2e119693eb1d4647bac8dceb57ff07db |
|---|
| Source note | uspto-grants-2007_03 |
|---|
