HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric acid magnesium salt (1:1) → HCID 86593167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 57939525 | HCID 57939525 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86593167 | HCID 86593167 | — |
Reaction Steps
Hydroxylamine hydrochloride (695 mg), sodium acetate (820 mg) and dry magnesium sulphate (500 mg) were added to a solution of intermediate 5b (500 mg) in dry MeOH (50 mL) under a Nitrogen atmosphere.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07196077B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-fd8c3762c3294048955a5e6d1925b14a |
| Source note | uspto-grants-2007_03 |