Formaldehyde → HCID 131726312, compound

Participants

Reaction Steps

A mixture of example 4 (10 mg), aqueous formaldehyde (29 μL) and 10% Pd/C (5 mg) in anhydrous MeOH (1 mL) was hydrogenated at r.t. and Patm. for 1 hour. The mixture was filtered and the organic layer was concentrated in vacuo. The residue was triturated with Et2O/pentane to give the title compound (5 mg) as a whitish solid.

Provenance & Evidence