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HRID460180

反应详情

EQUATION

反应方程式

HRID 460180 的结构方程式

REACTANTS

反应物

4
结构：S
HCID402

Hydrogen sulfide

H2S

结构：CCOC(=O)C(=O)CBr
HCID66144

Propanoic acid, 3-bromo-2-oxo-, ethyl ester

C5H7BrO3

结构：CC(C)(C)OC(=O)c1ccc(C#N)c(N)c1
HCID18771825

未命名化合物

结构：NS(=O)(=O)c1ccc(-c2nc(C(=O)O)cs2)cc1
HCID18772085

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)c1ccc(-c2nc(C(=O)O)cs2)c(N)c1
HCID69412598

未命名化合物

PROCEDURE

实验过程

In a manner similar to that described for the preparation of 2-(4-aminosulfonylphenyl)thiazole-4-carboxylic acid, 4-[(1,1-dimethylethoxy)carbonyl]-aminobenzonitrile was treated with H2S, ethyl bromopyruvate, and LIOH successively to give the title compound. MS m/z: 321 (M+H).