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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 460222Generated: October 30, 2026

HCID 18445337, compound → HCID 18771654, compound

https://huagongshe.com/reaction/460222

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18445337HCID 18445337—
CatalystPalladium hydroxideHCID 9942167—
SolventEthanolHCID 702—
ProductHCID 18771654HCID 18771654—

Reaction Steps

A solution of 1′-methyl-1′,2′,3′,6′-tetrahydro-[2,4′]bipyridinyl-6-ylamine (1.1 g, 5.8 mmol) and EtOH (30 mL) was hydrogenated over 20% Pd(OH)2/C (0.3 g) at 40 psi and RT. After 16 h, the mixture was filtered through Celite® and concentrated in vacuo to give the desired compound as a yellow solid. MS m/z: 192.1 (M+H). Calc'd for C11H17N3-191.27.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07196104B2
Source datasetuspto-grants-2007_03
ORD IDord-577d6e3bb5f7448f91dc08506bfb4070
Source noteuspto-grants-2007_03