HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → (s)-4-(8-Glycidyloxy-2h-chromen-3-ylcarbonyl)morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(8-hydroxy-2H-chromen-3-ylcarbonyl)morpholine | HCID 10563350 | — |
| Reactant | (S)-(+)-Glycidyl-4-nitrobenzoate | HCID 10868995 | — |
| Product | (s)-4-(8-Glycidyloxy-2h-chromen-3-ylcarbonyl)morpholine | HCID 60077970 | 77.3% |
Reaction Steps
By the reactions in the same manner as in Starting Material Synthesis Example 1 using 4-(8-hydroxy-2H-chromen-3-ylcarbonyl)morpholine (3.3 g), potassium carbonate (3.5 g) and (S)-glycidyl nosylate (3.3 g), the title compound (3.1 g) was obtained as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07196199B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-f99ee1041e41463988e99af2ee3c7ef9 |
| Source note | uspto-grants-2007_03 |