Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 361416 | HCID 361416 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69497811 | HCID 69497811 | — |
Reaction Steps
4-(2′-Methoxybenzylidene)-2-methyl-4H-oxazol-5-one (5 g) was dissolved in ethanol (100 ml) and an aqueous ethylamine solution (15 ml) and potassium carbonate (7 g) were added thereto. The mixture was heated at 80° C. for 5 hr. After cooling, the solvent was evaporated under reduced pressure and the precipitated yellow crystals were collected by filtration to give the title compound (1.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07196199B2 |
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| Source dataset | uspto-grants-2007_03 |
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| ORD ID | ord-426e205b5be049ff9d0fc599614c60e1 |
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| Source note | uspto-grants-2007_03 |
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