HRID460669

反应详情

EQUATION

反应方程式

HRID 460669 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

α-(2′-Hydroxybenzylidene)-γ-butyrolactone (5.0 g) was dissolved in ethanol (400 ml) and 10% palladium carbon (0.5 g) was added. The reaction mixture was reduced for 6 hr at 50 atm. The reaction mixture was filtered and the organic solvent was concentrated to give the title compound (5.0 g).

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered
  2. concentrationthe organic solvent was concentrated