Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(2-Hydroxybenzylidene)dihydrofuran-2(3h)-one → alpha-(2'-Hydroxybenzyl)-gamma-butyrolactone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(2-Hydroxybenzylidene)dihydrofuran-2(3h)-one | HCID 229758 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | alpha-(2'-Hydroxybenzyl)-gamma-butyrolactone | HCID 21813505 | 99% |
반응 단계
α-(2′-Hydroxybenzylidene)-γ-butyrolactone (5.0 g) was dissolved in ethanol (400 ml) and 10% palladium carbon (0.5 g) was added. The reaction mixture was reduced for 6 hr at 50 atm. The reaction mixture was filtered and the organic solvent was concentrated to give the title compound (5.0 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07196199B2 |
| 출처 데이터셋 | uspto-grants-2007_03 |
| ORD ID | ord-a898008607494e0f93fefb5ecfa45783 |
| 출처 메모 | uspto-grants-2007_03 |