HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 22762275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | N-[4-chloro-3-[[5-oxo-1-(2,4,6-trichlorophenyl)-4H-pyrazol-3-yl]amino]phenyl]tetradecanamide | HCID 178443172 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22762275 | HCID 22762275 | — |
Reaction Steps
A solution of 30.7 g (0.05 mole) of 1-(2,4,6-trichlorophenyl)-3-(2-chloro-5-myristoylamino-anilino)-2-pyrazolin-5-one and 15.6 g (0.1 mole) of phenyl chloroformiate in 100 ml of acetonitrile are refluxed for 4 h. The solution is poured out in water and the separated oil is stirred first with water and next with methanol. The precipitate is recrystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061498 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-be249b6a1114491a91def0ad79430d48 |
| Source note | uspto-grants-1977_12 |