HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 21394040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 22762272 | HCID 22762272 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21394040 | HCID 21394040 | — |
Reaction Steps
4.45 ml (0.055 mole) of sulfuryl chloride are added dropwise in 15 min at -50° C to a cooled solution of 34.4 g (0.05 mole) of 1-(2,4,6-trichlorophenyl)-2-ethoxycarbonyl-3-(2-chloro-5-myristoylamino-anilino)-3-pyrazolin-5-one (compound 19) in 100 ml dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061498 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-17dc7f76fe9d46519216082e0729e5e4 |
| Source note | uspto-grants-1977_12 |