Hydrochloric Acid → HCID 86735234, compound

HRID 460749Notes

Reaction equation

HRID 460749 reaction equation
[CH3:1][C@@:2]([C:8]([OH:10])=[O:9])([CH2:4][CH2:5][CH2:6][NH2:7])[NH2:3].[ClH:11]>>[ClH:11].[CH3:1][C@@:2]([C:8]([OH:10])=[O:9])([CH2:4][CH2:5][CH2:6][NH2:7])[NH2:3]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 1866402-Methyl-L-ornithine

Product 1

HCID 86735234HCID 86735234, compound

Procedure

An aqueous solution of 2-methyl-L-ornithine was adjusted to pH 5 with hydrochloric acid, concentrated and diluted with ethanol to yield 2-methyl-L-ornithine hydrochloride as prisms, 165 mg. (0.90 mmol, 73%) m.p. 222°-224° C.

Workup

  1. concentrationconcentrated
  2. additiondiluted with ethanol

Sources & evidence

ORD record
ord-0e973908fdee44f0a0081254097c0c88
Source dataset
uspto-grants-1977_12
Patent number
US04061542

Reaction notes

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