huagongshe.com
HRID460820

反应详情

EQUATION

反应方程式

HRID 460820 的结构方程式

REACTANTS

反应物

2
结构：CCNC(=S)NCC
HCID2735009

N,N'-Diethylthiourea

C5H12N2S

结构：NS(=O)(=O)c1cc(C(=O)CBr)c(Cl)cc1Cl
HCID22756429

未命名化合物

PRODUCTS

生成物

1
结构：Br.CCN=C1SCC(O)(c2cc(S(N)(=O)=O)c(Cl)cc2Cl)N1CC
HCID21394770

未命名化合物

PROCEDURE

实验过程

was obtained in a manner analogous to that described in Example 1 d) from 3.5 g of 2-bromo-2',4'-dichloro-5'-sulfamoyl-acetophenone and 1.3 g of 1,3-diethyl-thiourea. M.p. 202° C (decomposition).

WORKUP

后处理

  1. customwas obtained in a manner analogous to
  2. customthat described in Example 1 d