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HRID460821

反应详情

EQUATION

反应方程式

HRID 460821 的结构方程式

REACTANTS

反应物

2
结构：S=C(NC1CCCCC1)NC1CCCCC1
HCID727200

N,N'-Dicyclohexylthiourea

C13H24N2S

结构：NS(=O)(=O)c1cc(C(=O)CBr)c(Cl)cc1Cl
HCID22756429

未命名化合物

PRODUCTS

生成物

1
结构：Br.NS(=O)(=O)c1cc(C2(O)CSC(=NC3CCCCC3)N2C2CCCCC2)c(Cl)cc1Cl
HCID21394764

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

2.4 g of 1,3-dicyclohexyl-thiourea were added to 3,5 g of 2-bromo-2',4'-dichloro-5'-sulfamoylacetophenone in 40 ml of ethyl acetate. The whole was allowed to stand overnight at 20° C, the crystals were filtered off and washed with ethyl acetate. M.p. 161°-163° C.

WORKUP

后处理

  1. filtrationthe crystals were filtered off
  2. washwashed with ethyl acetate