HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Dicyclopropylthiourea → 4-(2,4-Dichloro-5-sulfamoylphenyl)-3-cyclopropyl-2-cyclopropylimino-1,3-thiazolidine-4-ol-hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Dicyclopropylthiourea | HCID 17750075 | — |
| Reactant | 2-Bromo-2',4'-dichloro-5'-sulfamoylacetophenone | HCID 22756429 | — |
| Product | 4-(2,4-Dichloro-5-sulfamoylphenyl)-3-cyclopropyl-2-cyclopropylimino-1,3-thiazolidine-4-ol-hydrobromide | HCID 21394792 | — |
Reaction Steps
was obtained in a manner analogous to that described in Example 10 from 3.5 g of 2-bromo-2',4'-dichloro-5'-sulfamoylacetophenone and 1.6 g of 1,3-dicyclopropyl-thiourea. M.p. 226° C (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061647 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-b60a71bba19d469eac652455f96bab82 |
| Source note | uspto-grants-1977_12 |