HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methyl-N'-phenethylthiourea → 4-(2,4-Dichloro-5-sulfamoylphenyl)-3-methyl-2-(2-phenylethylimino)-1,3-thiazolidine-4-ol-hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methyl-N'-phenethylthiourea | HCID 2725299 | — |
| Reactant | 2-Bromo-2',4'-dichloro-5'-sulfamoylacetophenone | HCID 22756429 | — |
| Product | 4-(2,4-Dichloro-5-sulfamoylphenyl)-3-methyl-2-(2-phenylethylimino)-1,3-thiazolidine-4-ol-hydrobromide | HCID 21394781 | — |
Reaction Steps
was obtained in a manner analogous to the method described in Example 10 from 3.5 g of 2-bromo-2',4'-dichloro-5'-sulfamoylacetophenone and 2 g of 1-methyl-3-(2-phenylethyl)-thiourea. M.p. 164°-165° C (decomposition)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061647 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-13cac9613dff408e8a7bec1e1731c764 |
| Source note | uspto-grants-1977_12 |