Thiourea, N,N'-di-2-propen-1-yl- → 3-Allyl-2-allylimino-(3,4-dimethyl-5-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide

HRID 460830Notes

Reaction equation

HRID 460830 reaction equation
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[C:9]([S:11](=[O:14])(=[O:13])[NH2:12])[C:8]([CH3:15])=[C:7]([CH3:16])[CH:6]=1)=[O:4].[CH2:17]([NH:20][C:21]([NH:23][CH2:24][CH:25]=[CH2:26])=[S:22])[CH:18]=[CH2:19]>>[BrH:1].[CH2:24]([N:23]1[C:3]([C:5]2[CH:10]=[C:9]([S:11](=[O:14])(=[O:13])[NH2:12])[C:8]([CH3:15])=[C:7]([CH3:16])[CH:6]=2)([OH:4])[CH2:2][S:22][C:21]1=[N:20][CH2:17][CH:18]=[CH2:19])[CH:25]=[CH2:26]

Participants

3

Reactant 2

HCID 3034186Thiourea, N,N'-di-2-propen-1-yl-HCID 213947832-Bromo-3',4'-dimethyl-5'-sulfamoylacetophenone

Product 1

HCID 213948103-Allyl-2-allylimino-(3,4-dimethyl-5-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide

Procedure

was obtained in a manner analogous to the method described in Example 6 in amorphous form from 3.1 g of 2-bromo-3',4'-dimethyl-5'-sulfamoyl-acetophenone and 1.6 g of 1,3-diallyl-thiourea and the substance was brought to crystallization under ether. M.p. 138°-140° C (decomposition).

Workup

  1. customwas obtained in a manner analogous to the method
  2. customthe substance was brought to crystallization under ether

Sources & evidence

ORD record
ord-69f0917013d143849cbcc32c600a02b4
Source dataset
uspto-grants-1977_12
Patent number
US04061647

Reaction notes

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