HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea, N,N'-di-2-propen-1-yl- → 3-Allyl-2-allylimino-(3,4-dimethyl-5-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea, N,N'-di-2-propen-1-yl- | HCID 3034186 | — |
| Reactant | 2-Bromo-3',4'-dimethyl-5'-sulfamoylacetophenone | HCID 21394783 | — |
| Product | 3-Allyl-2-allylimino-(3,4-dimethyl-5-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide | HCID 21394810 | — |
Reaction Steps
was obtained in a manner analogous to the method described in Example 6 in amorphous form from 3.1 g of 2-bromo-3',4'-dimethyl-5'-sulfamoyl-acetophenone and 1.6 g of 1,3-diallyl-thiourea and the substance was brought to crystallization under ether. M.p. 138°-140° C (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061647 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-69f0917013d143849cbcc32c600a02b4 |
| Source note | uspto-grants-1977_12 |