HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21395230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Chloro-2-(diethylamine)ethane hydrochloride | HCID 13363 | — |
| Reactant | N-4-Piperidylbenzamide | HCID 118120 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 21395230 | HCID 21395230 | — |
| Product | HCID 131710748 | HCID 131710748 | — |
Reaction Steps
Equimolar amounts of 2-diethylaminoethyl chloride, hydrochloride and 4-benzamidopiperidine were stirred under reflux in isopropanol with 2.5 molar equivalents of anhydrous potassium carbonate for 18 hours. The hot suspension was filtered and the filtrate was treated with ethereal HCl to give the title compound as a dihydrochloride, hemihydrate, m.p. >220° (with decomp.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061758 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-cf130ce939d641f5b057effd84a5efbe |
| Source note | uspto-grants-1977_12 |