HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 23455198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Theophylline | HCID 2153 | — |
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Product | HCID 23455198 | HCID 23455198 | 78.2% |
Reaction Steps
A suspension of 3.60 g (0.02 mole) of theophylline, 2.30 g (0.02 mole) of pyridine hydrochloride and 0.7 g (0.023 mole) of paraformaldehyde was heated at 80° for 24 hr. Upon cooling, crystals immediately formed in the solution. The crystals were filtered and dried in vacuo to give 4.83 g (28% yield) of the desired compound as its hydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061753 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-09a9bf2ad8f542c58e4a6927355828e6 |
| Source note | uspto-grants-1977_12 |