HuagongsheHuagongshe Chemistry Print Report · For research reference only
2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- → HCID 178478542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- | HCID 75657 | — |
| Reactant | 2-(4-Chlorophenyl)ethan-1-amine--hydrogen chloride (1/1) | HCID 12251519 | — |
| Product | HCID 178478542 | HCID 178478542 | — |
Reaction Steps
A slurry of 15.9 g (0.08 mole) of p-chlorophenethylamine hydrochloride in 25 ml of O-methylcaprolactim is allowed to stand at room temperature 3 days with occasional stirring with a glass rod. The mixture is then cooled and the resulting solid is collected, washed with ether and recrystallized from methanol-acetone to give 2-(p-chlorophenylethylimino)hexahydroazapine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061746 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-5b278b0be4584379833361726e6a865c |
| Source note | uspto-grants-1977_12 |