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HRID461119

反应详情

EQUATION

反应方程式

HRID 461119 的结构方程式

REACTANTS

反应物

2
结构：NS(=O)(=O)c1cc(C(=O)CBr)ccc1Cl
HCID12952390

未命名化合物

结构：CCNC(=S)NC(C)C
HCID19650595

未命名化合物

PRODUCTS

生成物

1
结构：CCN1C(=NC(C)C)SCC1(O)c1ccc(Cl)c(S(N)(=O)=O)c1.Cl
HCID22760539

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

6.2 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone and 2.92 g of 1-ethyl-3-isopropylthiourea were heated in 40 ml of acetone for 15 minutes to 40° C, the mixture was stirred for another 30 minutes at room temperature and the crystals were filtered.

WORKUP

后处理

  1. filtrationthe crystals were filtered