Diethyl Ether → HCID 22760541, compound

HRID 461120Notes

Reaction equation

HRID 461120 reaction equation
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH:16]([NH:20][C:21]([NH:23][CH:24]([CH2:26][CH3:27])[CH3:25])=[S:22])([CH2:18][CH3:19])[CH3:17].C(OCC)C>C(OCC)(=O)C>[ClH:1].[CH:24]([N:23]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:22][C:21]1=[N:20][CH:16]([CH2:18][CH3:19])[CH3:17])([CH2:26][CH3:27])[CH3:25]

Participants

5

Reactant 3

HCID 3283Diethyl EtherHCID 5366322N,N-Di-sec-butylthioureaHCID 213167492,4'-Dichloro-3'-sulfamoylacetophenone

Product 1

HCID 22760541HCID 22760541, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

5.3 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 3.8 g of 1,3-di-sec.-butylthiourea were reacted in the manner described in Example 16, the reaction was introduced into a solution of 40 ml of diethyl ether and 120 ml of ethyl acetate and the colorless, crystalline end product was filtered off after stirring for 4 hours at room temperature.

Workup

  1. filtrationthe colorless, crystalline end product was filtered off

Sources & evidence

ORD record
ord-8526a8136bbe4a5c9de09aca16c3d3fa
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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