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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 461144Generated: October 30, 2026

N-Methyl-N'-[(pyridin-2-yl)methyl]thiourea → HCID 22760667, compound

https://huagongshe.com/reaction/461144

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-Methyl-N'-[(pyridin-2-yl)methyl]thioureaHCID 12629156—
Reactant2,4'-Dichloro-3'-sulfamoylacetophenoneHCID 21316749—
ProductHCID 22760667HCID 22760667—

Reaction Steps

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 3.5 g of 1-methyl-3-(2-pyridylmethyl)-thiourea were reacted as prescribed in Example 12 and the end product was precipitated with 400 ml of ethyl acetate while stirring. Colorless crystals, melting point 152° C (decomposition) γC=N 1620 cm-1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04061761
Source datasetuspto-grants-1977_12
ORD IDord-613d4b1851a34368981151a893623baf
Source noteuspto-grants-1977_12