HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → 4'-Methyl-3'-sulfamoyl-diazoacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 4-Methyl-3-sulfamoyl-benzoyl chloride | HCID 22760560 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 4'-Methyl-3'-sulfamoyl-diazoacetophenone | HCID 54047535 | — |
Reaction Steps
12 g of 4-methyl-3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the substance precipitating as fair yellow precipitate was filtered off. Melting point: 176° C (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-d01df7b968fc4bda8abbeb8f76885435 |
| Source note | uspto-grants-1977_12 |