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HRID461154

反应详情

EQUATION

反应方程式

HRID 461154 的结构方程式

REACTANTS

反应物

2
结构：C=[N+]=[N-]
HCID9550

Diazomethane

CH2N2

结构：Cc1ccc(C(=O)Cl)cc1S(N)(=O)=O
HCID22760560

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(C(=O)C=[N+]=[N-])cc1S(N)(=O)=O
HCID54047535

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

12 g of 4-methyl-3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the substance precipitating as fair yellow precipitate was filtered off. Melting point: 176° C (decomposition).

WORKUP

后处理

  1. customthe substance precipitating as fair yellow precipitate
  2. filtrationwas filtered off